Synopsis
ID02 beamline is a combined ultra small-angle and wide-angle scattering instrument. The microstructure and non-equilibrium dynamics of soft matter and related systems can be probed from sub-nanometer to micron scale, and down to sub-millisecond time range.
Status:
open
Disciplines
- Life Sciences
- Physics
- Chemistry
- Materials and Engineering
- Environmental Sciences
- Medicine
Applications
- Soft condensed matter
- Noncrystalline structural biology
- Interdisciplinary areas of soft matter, biology, and nanoscience
Techniques
-
SAXS - small-angle X-ray scattering
-
USAXS - ultra-small-angle X-ray scattering
-
WAXS - wide-angle X-ray scattering
-
USA-XPCS - ultra-small-angle XPCS
-
Time-resolved USAXS
-
Time-resolved SAXS
Beam size
- Minimum (H x V) : 20.0
x 20.0
µm²
-
Maximum (H x V) : 1000.0
x 60.0
µm²
Sample environments
- Stopped-flow rapid mixing device
- Stress controlled rheometer
- Fast pressure-jump setup
- Mettler heating stage (FP90/FP84HT)
- Linkam heating stage: (THMS600/TMS94)
- Peltier-controlled flow-through capillary cell
- Magnetic field (0.1 mT to 1.5 T)
- Oven (capillaries and flat cells, 25-300°C)
- Peltier-controlled automatic sample changer
Detectors
- SAXS: Rayonix MX170
- SAXS: Pilatus 300K
- WAXS: Rayonix LX170
- USAXS: FReLoN Kodak CCD
- XPCS: Eiger 500K
Technical details
COMBINED USAXS/SAXS/WAXS: ID02 offers time-resolved ultrasmall-, small- & wide- angle X-ray scattering (combined USAXS/SAXS/WAXS) capabilities. The setup uses a monochromatic, highly collimated, and intense beam in the pinhole configuration with sample-to-detector distance variable from 0.8 m to 31 m. The collimation is usually achieved using slits but the high resolution USAXS configuration may also employ a double crystal collimation scheme to reduce the horizontal beam divergence. Using 1 Å X-ray wavelength, the q range covered by the instrument is roughly 10-3 nm-1< q < 60 nm-1.
More detailed information about the scattering techniques, sample environments, and detectors is available at the beamline home page, which also lists recent publications illustrating the capababilities of the instrument. An up-to-date reference for the beamline technical specifications and performance is the following [1]. Please note that the beamline web page is not a reference and the link is subject to change.
[1] T. Narayanan, M. Sztucki, P. Van Vaerenbergh, J. Le´onardon, J. Gorini, L. Claustre, F. Sever, J. Morse and P. Boesecke, J. Appl. Cryst., 51, 1511 (2018); https://doi.org/10.1107/S1600576718012748.
Different instrumental approaches to understand the chitosan coated niosomes/mucin interaction
Rinaldi F., Hanieh P.N., Imbriano A., Passeri D., Del Favero E., Rossi M., Marianecci C., De Panfilis S., Carafa M.,
Journal of Drug Delivery Science and Technology 55, 101339-1-101339-9 (2020)
Layered organization of anisometric cellulose nanocrystals and beidellite clay particles accumulated near the membrane surface during cross-flow ultrafiltration: In situ SAXS and ex situ SEM/WAXD characterization
Semeraro E.F., Hengl N., Karrouch M., Michot L.J., Paineau E., Jean B., Putaux J.L., Lancelon-Pin C., Sharpnack L., Pignon F.,
Colloids and Surfaces A: Physicochemical and Engineering Aspects 584, 124030-1-124030-12 (2020)
Effect of calcium ions and disulfide bonds on swelling of virus particles
Asor R., Khaykelson D., Ben-nun-Shaul O., Oppenheim A., Raviv U.,
ACS Omega 4, 58-64 (2019)
Assembly reactions of hepatitis B capsid protein into capsid nanoparticles follow a narrow path through a complex reaction landscape
Asor R., Selzer L., Schlicksup C.J., Zhao Z.C., Zlotnick A., Raviv U.,
ACS Nano 13, 7610-7626 (2019)
Effects of a cationic surfactant incorporation in phytantriol bulk cubic phases and dispersions loaded with the anticancer drug 5-fluorouracil
Astolfi P., Giorgini E., Adamo F.C., Vita F., Logrippo S., Francescangeli O., Pisani M.,
Journal of Molecular Liquids 286, 110954-1-110954-7 (2019)
Gum Arabic in solution: Composition and multi-scale structures
Atgié M., Garrigues J.C., Chennevière A., Masbernat O., Roger K.,
Food Hydrocolloids 91, 319-330 (2019)