Nano calorimeter

Temperature range: RT to 450°C (can be shifted using add. equipment)
Heating rates: 0-180K/min (AC-Mode), 35-20'000K/s (Burst Mode, < 10 s duration)
Buffer: 2 mega-samples; Sampling rate: up to 40khz

Sample: solid; sample mass < 0.5µg
max sample size < 60 x 60 x 15 µm³

Xray-technique: suitable for transmission geometries; partially compatible with reflection geometry

Special introduction to the functioning of the device is required, MEMS need to be calibrated before use (to be done in collaboration with the beamline personel)

(1) Square hole pattern (M3) 40 x 40 mm raster (height to beam 30mm)
(2) Square hole pattern (M2) 14 x 14 mm raster (height to beam 82mm)

MEMS nano-heater / Nano calorimeter

Nano calorimeter on the BL

ID13 - MICROFOCUS BEAMLINE