Time Resolved Publications

see also highlights list
 
 
 

2005

"Thermal dynamics in laser excited metal nanoparticles"
A. Plech, V. Kotaidis, M. Lorenc, M. Wulff
Chemical Physics Letters 401, 565-569, 2005.

"Picosecond x-ray studies of coherent folded acoustic phonons in a multiple quantum well"
P. Sondhauss, J. Larsson, M. Harbst, G.A. Naylor, A. Plech, K. Scheidt, O. Synnergren, M. Wulff, and J.S. Wark
Physical Review Letters 94, 125509, 2005.

"Time-resolved X-ray diffraction: a wonderful tool for probing structural photo-induced phase transitions"
M.Buron-Le Cointe, E. Collet, L. Guerin, M.H. Lemee-Cailleau, H. Cailleau, M.Wulff, T. Luty, S. Koshihara, K. Tanaka
Journal of Luminescence 112, 235-241, 2005

"Ultrafast X-ray Diffraction of Transient Structures in Solution"
H. Ihee, M. Lorenc, T. K. Kim, Q. Y. Kong, M. Cammarata, J. H. Lee, S. Bratos, M. Wulff
Science 309, 1223-1227, 2005. See also commentary by P. Anfinrud & F. Schotte, "X-ray Fingerprinting of Chemical Intermediates in Solution", Science 309, 1192-1193, 2005

"Structural Determination of a Transient Isomer of CH2I2 by Picosecond X-Ray Diffraction"
J. Davidsson, J. Poulsen, M. Cammarata, P. Georgiou, R. Wouts, G. Katona, F. Jacobson, A. Plech, M. Wulff, G. Nyman and R. Neutze
Physical Review Letters 94, 245503, 2005.

"Visualizing Reaction Pathways in Photoactive Yellow Protein from Nanoseconds to Seconds"
H. Ihee, S. Rajagopal, V. ?rajer, R. Pahl, S. Anderson, M. Schmidt, F. Schotte, P. A. Anfinrud, M. Wulff, K. Moffat
PNAS 102, 7145-7150, 2005.

2004

"Probing photo induced phase transition in a charge-transfer molecular crystal by 100 picosecond X-ray diffraction"
L. Guerin, E. Collet, M.-H. Lemee-Cailleau, M. Buron-Le Cointe, H. Cailleau, A. Plech, M. Wulff, S.-Y. Koshihara and T. Luty
Chemical Physics, 299, 163-170, 2004

"Visualising Chemical Reactions in Solution by Picosecond X-ray Diffraction"
Plech, M. Wulff, S. Bratos, F. Mirloup, R Vuilleumier, F. Schotte and P.A. Anfinrud
Physical Review Letters, 92, 125505-1 to 125505-4, 2004. Commentary by Stuart Rice, Nature, 429, 255, 2004

"Time-dependent x-ray scattering signal of laser heated liquids"
F. Mirloup, R. Vuilleumier, S. Bratos, M. Wulff and A. Plech
Published in the book "Femtochemistry and Femtobiology: Ultrafast Events in Molecular Science". Editors: Monique M. Martin and James T. Hynes, Elsevier, p 349-352, 2004

"Time-resolved x-ray diffraction from small molecules in solution"
M. Wulff, M. Lorenc, A. Plech, H. Ihee, S. Bratos, F. Mirloup and R. Vuilleumier
Published in the book titled "Femtochemistry and Femtobiology: Ultrafast Events in Molecular Science". Editors: Monique M. Martin and James T. Hynes, Elsevier, p 337-347, 2004

"Chromophore Conformation and the Evolution of Tertiary Structural Changes During the Photocycle of Photoactive Yellow Protein"
S. Anderson, V. Srajer, R. Pahl, S. Rajagopal, F. Schotte, P. Anfinrud, M. Wulff and K. Moffat
Structure, 12, 1039-1045, 2004.

"X-ray Filming of atomic motions in chemical reactions"
S. Bratos, F. Mirloup, R. Vuilleumier, M. Wulff and A. Plech
Chemical Physics, 304, 245 -251, 2004.

"Picosecond Time-Resolved X-ray Crystallography: Probing Protein Function in Real Time"
Friedrich Schotte, Jayashree Soman, John S. Olson, Michael Wulff, and Philip A. Anfinrud
Journal of Structural Biology. Special issue: Time-Resolved Imaging of Macromolecular Processes and Interactions - Edited by Joachim Frank and Ilme Schlichting, Vol 147/3 pp 235-246, 2004.

"Time Resolved X-ray Diffraction and Non-Thermal Inelastic X-ray Scattering"
P. Sondhauss,, M. Harbst, J. Larsson, G.A Naylor, A. Plech, K. Scheidt, O. Synnergren, J.S. Wark, M. Wulff
In AIP conference proceedings 705, 1387-90, 2004.

2003

“Time-resolved X-ray diffraction on laser excited metal nanoparticles” A. Plech, S. Kuerbitz, K.-J. Berg, H. Graener, G. Berg, , S. Grésillon, M. Kaempfe, J. Feldmann, M. Wulff and G. von Plessen.
Europhys.Lett., 61 (6), 762-768, 2003

“Structure determinations in liquid solutions – implications for picosecond photo-excitation studies”
A. Plech, R. Randler, M. Wulff, F. Mirloup, R. Vuilleumier.
Journal of Physics: Condensed Matter 15, S137-S143, 2003

“Watching a protein as it functions: real-time observations using picosecond crystallography”
F. Schotte, P. Anfinrud, M. Wulff and D. Bourgeois.
Published in: R. Dwayne Miller, Margareth M. Murnane, Norbert F. Scherer, Andrew M. Weiner (Eds.), "Ultrafast Phenomena XIII", Proceedings of the 13th International Conference, Vancouver, BC, Canada, May 12-17, 2002, Spinger Verlag, Belin/Heidelberg, ISBN 3-540-00089-5, 2003

“Laser-Induced Ferroelectric Structural Order in an Organic Charge-Transfer Crystal”
E. Collet, M. H. Lemée-Cailleau, M. Buron-Le Cointe, H. Cailleau, M. Wulff, T. Luty, S.Y. Koshihara, M. Meyer, L. Toupet and P. Rabiller, S. Techert
Science, 300, 612-615, 2003.
See also commentary by Craig W. Siders and Andrea Cavalleri, Science, 300, 591-592, 2003

“Watching a Protein as it Functions: 150 ps Time-resolved Structures of a Myoglobin Mutant at 1.7 Å Resolution”
F. Schotte, M. Lim, T. A. Jackson, A. Smirnov, J. Soman, J. S. Olson, G. N. Phillips, M. Wulff, and P. A. Anfinrud.
Science, 300, 1944-1947, 2003
See also commentary “ A Picosecond Resolution Crystallographic Movie, Stephen G. Benka, Physics Today, September, p9, 2003

“A new apparatus for the measurement of X-ray absorption by flame generated particles”
J.B.A. Mitchell, J.L. LeGarrec, D. Travers, B.R. Rowe, R.J. Randler, A. Plech, M. Wulf
Nuclear Instruments and Methods in Physics Research B 207, 227–231, 2003

“Real time visualization of atomic motions in dense phases”
S. Bratos, J.CL. Leicknam, F. Mirloup, R. Vuilleumier, G. Gallot, M. Wulff, A. Plech and S. Pommeret
In book edited by C. Samios “ Novel Approaches to the Structure and Dynamics of Liquids: Experiments, Theories and Simulations, Kluwer Academic Publishers, Netherlands, p 111-128, (2004).

“Complex landscape of protein structural dynamics unveiled by nanosecond Laue crystallography”
D. Bourgeois, B. Vallone, F. Schotte, P. Anfinrud, M. Wulff, M. Brunori
PNAS, 100, no 15, 8704–8709, 2003
See also commentary by H. Frauenfelder, B. H. McMahon and P. W. Fenimore: Myoglobin: The hydrogen atom of biology and a paradigm of complexity PNAS, 100, no. 15, 8615–8617, 2003

“Performance of a cryogenically cooled monochromator: FEA predictions compared with experimental measurements"
L. Zhang, W.-K. Lee, M. Wulff, L. Eybert
J. Synchrotron Rad. 10, 313–319, 2003

“Characterization of photocycle intermediates in crystalline photoactive yellow protein”
Remco Kort, Raimond B. Ravelli, Friedrich Schotte, Dominique Bourgeois, Wim Crielaard, Klaas J. Hellingwerf and Michael Wulff
Journal Photochemistry Photobiology, 78(2), 131-137, 2003

2002

"The realization of sub-nanosecond pump and probe experiments at the ESRF"
M. Wulff,  A.  Plech, L.  Eybert, R.  Randler, F. Schotte and P. Anfinrud,
Faraday Discussions 122 (2002) .

"Time-resolved and static-ensemble structural chemistry of hydroxymethylbilane synthase"
J. R. Helliwell, Y. P. Nieh, J.  Habash, P.  F. Faulder, J.  Raftery, M.  Cianci, M. Wulff and  A. Hädener,
Faraday Discussions 122 (2002) .

"Nanosecond time-resolved crystallography of photo-induced species: case study and instrument development  for high-resolution excited-state single-crystal structure determination"
J. M. Cole, P. R. Raithby, M. Wulff, F.  Schotte, A. Plech, S.  J. Teat and G. Bushnell-Wye,
Faraday Discussions 122 (2002) .

"First investigations of the kinetics of the topochemical reaction of p-formyl-trans-cinnamic acid by time-resolved X-ray diffraction"
G. Busse, T. Tschentscher, A. Plech, M. Wulff, B. Frederichs and S. Techert,
Faraday Discussions 122 (2002) .

"Diffuse scattering from liquid solutions with white-beam undulator radiation for photoexcitation studies"
A. Plech, R. Randler, A. Geis and M. Wulff,
J. Synchr. Rad. 9 (2002) 287.

"Time-resolved x-ray diffraction: Statistical theory and its application to the photo-physics of molecular iodine"
S. Bratos, F. Mirloup, and R. Vuilleumier and M. Wulff,
J. Chem. Phys. 116 (2002) 10615.

"Recent advances in the generation of pulsed synchrotron radiation suitable for picosecond Time-resolved  X-ray studies"
F. Schotte, S. Techert, P.A. Anfinrud, V. Srajer, K. Moffat and M. Wulff,
In the book titled "Third-Generation Hard X-ray Synchrotron Radiation Sources", Edited by Dennis Mills, ISBN 0-471-31433-1 2002 John Wiley & Sons, Inc.

2001

"Direct time-resolved studies of photochemical reactions in liquids by X-ray scattering"
A. Geis, M. Bouriau, A. Plech, F. Schotte, S. Techert, H.P. Trommsdroff, M. Wulff and D. Block,
Journal of Luminescence 94–95 (2001) 493–498.

"A sub-picosecond accumulating streak camera for x-rays"
G.A.Naylor, K. Scheidt, J.Larsson, M.Wulff, and J.M.Filhol,
Meas. Sci. Technol. 12 (2001) 1858-1864.

Les "caméras à molécules" observent les protéines en plein travail
"Nous pouvons filmer en temps réel les transformations et les mouvements des protéines"
Le Monde from 09/11/2001.

"Molecular Movie at 1.8 A Resolution Displays the Photocycle of Photoactive Yellow Protein, a Eubacterial Blue-light Receptor, from Nanoseconds to Seconds"
Zhong Ren, Benjamin Perman, Vukica Srajer, T.-Y Teng, Claude Pradervand, Dominique Bourgeois, Friedrich Schotte, Thomas Ursby, Michael Wulff, Remco Kort, Klaas Hellingwerf, Keith Moffat,
Biochemistry; vol. 40 (2001) 13788-13801

"Protein Conformational Relaxation and Ligand Migration in Myoglobin: A Nanosecond to Millisecond Molecular Movie from Time-Resolved Laue X-ray Diffraction"
Vukica Srajer, Zhong Ren, Tsu-Yi Teng, Marius Schmidt, Thomas Ursby, Dominique Bourgeois, Claude Pradervand, Wilfried Schildkamp, Michael Wulff and Keith Moffat,
Biochemistry (2001)  vol. 40 (2001) 13802-13815.

"Visualizing Photochemical Dynamics in Solution through Picosecond X-ray Scattering"
Richard Neutze, Remco Wouts, Simone Techert, Jan Davidsson, Menhard Kocsis, Adam Kirrander, Friedrich Schotteand Michael Wulff
Phys. Rev. Lett 87 (2001) 195508 1-4 .

"Ultrafast x-ray diffraction tracks molecular shape-shifting"
C. Day; about below PRL,
0 Physics Today 54(3) (2001) 19.

“Picosecond X-ray Diffraction Probed Transient Structural Changes in Organic Solids”
S. Techert, S., Schotte, F., Wulff, M.
Physical Review Letters 86(9) (2001) .
 
 

2000

“Generation of short pulses of hydroxyl radicals by synchrotron radiation for time-resolved hydroxyl radical footprinting”
Roessle, M., Zaychikov E., Denissoval L., Wulff, M.,  Schotte, F., Hanfland, M., Sclavi, B., Badaut, C., Buckle, M., Heumann, H.
ESRF Newsletter  34 (2000) 24-26.

“Towards automated Laue data processing: application to the choice of optimal X-ray spectrum”
Bourgeois, D., Wagner, U., Wulff, M.
Acta Crystallographica Section D 56(8) (2000) 973-985.

“Extraction of accurate structure-factor amplitudes from Laue data: wavelength normalization with wiggler and undulator X-ray sources”
Srajer, V. Crosson, S. Schmidt, M. Key, J. Schotte, F. Anderson, S. Perman, B. Ren, Z. Teng, T. Y. Bourgeois, D.
Journal of Synchrotron Radiation 7(4) (2000)  236-244 .
 

1999

“Accurate and highly complete synchrotron protein Laue data using ESRF CCD and the Daresbury Laue software”
Nieh, Y. P., Raftery, J., Weisgerber, S., Habash, J.,  Schotte, F., Ursby, T., Wulff, M., Hadener, A., Campbell, J. W.,  Harding, M.M., Helliwell, J. R.,
Journal of  Synchrotron Radiation 6 (1999) 995-1006.
 

“Time Resolved experiments in the Picosecond to Microsecond Range using Pulsed Synchrotron
Radiation”
F. Schotte, F., Techert, S., Anfinrud, P. A., Srajer, V., Moffat, K., Wulff, M.
Proceeding of the ‘Workshop on the development of future electron-positron colliders for particle physics and for research using free electron lasers, Lund 23-25 September 1999, CERN Geneva, Nov. (1999) 207-227.

1998

"Time-resolved structures of hydroxymethylbilane synthase(Lys59Gln mutany) as it is loaded with substrate in the crystal determined by Laue diffraction”
Helliwell, J. R., Nieh, Y. P., Raftery J., Cassetta A., Habash J., Carr, P. D. , Ursby, T., Wulff, M., Thompson, A. W., Niemann, A.C., Hadener, A.
Journal of the Chemical Society-Faraday Transactions  94(17) (1998) 2615-2622.
 
 

T. E. Meyer, G. Tollin, M. A. Cusanovich, Benjamin Perman, Michael Wulff, Klaas Hellingwerf,and Keith
Moffat,
Science 1998 September 25; 281: 1961
 

“An integration routine based on profile fitting with optimized fitting area for the evaluation of  weak and/or overlapped 2-dimensional Laue or monochromatic patterns”
Bourgeois, D., Nurizzo, D., Kahn, R.,  Cambillau, C.,
Journal of Applied Crystallography 31 (1998) 22-35.

“X-ray brightness gets a boost”
M. Altarelli, M., Schlacter, F., Cross, J.
Scientific American 12 (1998) 66-73.

“Laser and synchrotron radiation pump-probe x-ray absorption experiment with sub-ns resolution”
Bressler, C. Chergui, M. Pattison, P. Wulff, M.
Proceedings- SPIE The International Society for Optical Engineering 3451  (1998) 108-116.
 

“Energy Transduction on the Nanosecond Time Scale: Early Structural Events in a Xanthopsin Photocycle”
Perman, B. Srajer, V. Ren, Z. Teng, T.-Y. Pradervand, C. Ursby, T. Bourgeois, D. Schotte, F. Wulff, M. Kort, R.
Science 5358 (1998) 1946-1949
 

1997

“The Realisation of 100 psec Laue Diffraction on ID09 and Shortcuts to 100 fsec Time Resolution in x-ray
Scattering Experiments”
Wulff, M., Bourgeois,  D., Ursby, T., Goirand, L., Mourou, G.
Published in "Time-Resolved Diffraction", editors J. R.Helliwell and P. M. Rentzepis, Clarendon Press, Oxford (1997) 195-228.

“Time-resolved protein crystal diffraction: determination by the Laue method of the behavior of the
enzyme hydroxymethylbilane systhase(LYS59Gln mutant) as it loaded with substrate in the crystal”
Helliwell, J.R., Nieh, Y. P., Casetta, A., Raftery, J., Hadener, A., Niemann, A.C., Battersby, A.R., Carr,
P.D., Wulff, M., Ursby, T., Moy, J. P., and Thompson, A.W.
Published in "Time-Resolved Diffraction", editors J. R.Helliwell and P. M. Rentzepis, Clarendon Press, Oxford (1997) 187-194.

“Laue and monochromatic technique developments for time-resolved biological and pertubation chemical
crystallography”
Bradbrook, G., Deacon, A., Habash, J., Helliwell, J.R., Helliwell, M., Nieh, Y. P., Raftery, J., Snell, E.H., Trapani, S., Thompson, A.W., Moon, K., Ursby, T., Wulff, M.
Published in "Time-Resolved Diffraction", editors J. R.Helliwell and P. M. Rentzepis, Clarendon Press, Oxford (1997) 166-186.

“Improved Estimation of Structure Factor Difference Amplitudes from Poorly Accurate Data”
Ursby, T., Bourgeois, D.
Acta Crystallographica A53 (1997) 564-575

“Time-resolved structures of macromolecules at the ESRF: Single-pulse Laue diffraction, stroboscopic data collection and femtosecond flash photolysis”
Wulff, M. Schotte, F. Naylor, G. Bourgeois, D.
Nuclear Instruments and Methods in Physics Research Section A 398(1) (1997) 69-84.
 

“Accuracy of Structural Information Obtained at the European Synchrotron Radiation Facility from Very Rapid Laue Data Collection on Macromolecules”
Bourgeois, D. Longhi, S. Wulff, M. Cambillau, C.
Journal of Applied Crystallography 30(2) (1997) 153-163.

“Time Resolved Biological and Perturbation Chemical Crystallography: Laue and monochromatic
Developments “
G. Bradbrook, A. Deacon, J. Habash, J. R. Helliwell, Y.P. Nieh, E. H. Snell, S. Trapani, A.W. Thompson, J. W. Campbell, N. M. Allison, K. Moon, T. Ursby and M. Wulff,
Published in "Time-Resolved Diffraction", editors J. R.Helliwell and P. M. Rentzepis, Clarendon Press, Oxford (1997) 166-186.
 

1996

“Nanosecond Crystallographic Snapshot of Protein Structural Changes”
W. A. Eaton, E. R. Henry, J Hofrichter,
SCIENCE 274 (1996) 1631-1632.

“Single-Pulse Laue Diffraction, Stroboscopic Data Collection and Femtosecond Flash Photolysis on
Macromolecules”
M. Wulff, F. Schotte, G. Naylor, D. Bourgeois, K. Moffat and G. Mourou
AIP Conference Proceedings, X-ray and Inner-Shell Processes, Hamburg 389 (1996) 267-293.

“Photolysis of the Carbon Monoxide Complex of Myoglobin: Nanosecond Time-Resolved Crystallography”
Srajer, V. Teng, T.-Y. Ursby, T. Pradervand, C. Ren, Z. Adachi, S.-I. Schildkamp, W. Bourgeois, D. Wulff, M. Moffat, K.
Science  5293 (1996) 1726-1728.
 

“New opportunities for time resolved X-ray scattering at the ESRF”
Wulff, M. Ursby, T. Bourgeois, D. Schotte, F. Zontone, F. Lorenzen, M.
journal de Chimie Physique et de Physico Chimie Biologique 93(10) (1996) 1915-1937.
 

“The structure of the Escherichia coli EF-TuùEF-Ts complex at 2.5 resolution”
Kawashima, T. Berthet-Colominas, C. Wulff, M. Cusack, S. Leberman, R.
Nature  6565 (1996)  511-518

“Feasibility and Realization of Single-Pulse Laue Diffraction on Macromolecular Crystals at  ESRF”
Bourgeois, D. Ursby, T. Wulff, M. Pradervand, C. Legrand, A. Schildkamp, W. Laboure, S. Srajer, V. Teng, T. Y. Roth, M.
journal of Synchrotron Radiation 3(2) (1996) 65-74.

“Trends and Challenges in Experimental Macromolecular Crystallography”
N. E. Chagen, T.J. Boggon, A. Casetta, A. Deacon, T. Gleichmann, J. Habash, S.J. Harrop, J.H. Helliwell, Y.P. Nieh M. Peterson J. Raftery, E.H. Snell, V. Stojanoff, A.W. Thompson T. Ursby and M. Wulff,
Quarterly Review of Biophysics 29(3) (1996)  227-278.

1995

“Experience from a Cryogenically Cooled Diamond Crystal Monochromator”
H. Yamaoka, A. K. Freund, J. Holmberg, M. Rossat, M. Wulff, M. Hanfland, W.-K Lee and D. M. Mills
Nuclear Instruments and Methods in Physics Research A 364 (1995) 581-584.

“High Heat Load Performance of a Liquid Nitrogen Cooled Thin Silicon Crystal Monochromator on a
High-Power Focused Wiggler Synchrotron Beam”
C. S. Rogers, D. M. Mills, W. K. Lee, G. Knapp, A. Freund, M. Wulff, H.Holmberg, M. Rossat, M. Hanfland, H. Yamaoka
Reviev of  Scientific Instruments  66(6) (1995) 3494.
 

“Single Pulse Laue Images from Macromolecular Crystals Recorded at ESRF”
D. Bourgeois, T. Ursby, M. Wulff, C. Pradervand, V. Srajer, A. Legrand, W. Schildkamp, S. Labouré, C. Rubin, T.Y. Teng, M. Roth and K. Moffat,
SPIE Proceedings on "Time-Resolved Electron and X-ray Diffraction",13-14 July, San Diego, 2521 (1995) 178-181,

“The Realization of Fast Diffraction on BL3 at the ESRF”
M. Wulff, T. Ursby, D. Bourgeois, L. Goirand, M. Sánchez del Río,
SPIE Proceedings on "Time-Resolved Electron and X-ray Diffraction",13-14 July, San Diego, 2521 (1995)197-206.
 

1994

Performance of diamond as X-ray monochromator under very high heat flux in a synchrotron  beam
Als-Nielsen, J. Freund, A. K. Wulff, M. Hanfland, M.
Nuclear Instruments and Methods in Physics Research Section B 94(3) (1994) 348.